A Low Temperature Single Crystal X-Ray Diffraction Technique

Abstract

A low temperature x‐ray diffraction technique, especially suitable to single crystal work, is described. Crystals are grown in glass capillaries on the x‐ray camera. Position and orientation are determined with the aid of a polarizing microscope on the apparatus. A special specimen holder is used which prevents moisture condensation and permits rotation and oscillation of the specimen while it is being cooled.