An Improved Hydride Generation-Atomic Absorption Apparatus for Selenium Determination
- 1 May 1975
- journal article
- spectroscopy
- Published by Taylor & Francis in Analytical Letters
- Vol. 8 (5), 323-337
- https://doi.org/10.1080/00032717508058214
Abstract
A hydrogen-flushed hydride generation utilizing a 1 % solution of NaBH4 as a reductant is wed with a non-heated quartz tube atomizer for selenium determination in feed and forage samples. A small amount of oxygen is added to the hydrogen to support combustion and atomization of the hydride. The sensitivity is 6 × 10−10 g. with linear analytical curves and good accuracy. The relative standard deviation of the method is 5–8 %.Keywords
This publication has 4 references indexed in Scilit:
- Flameless Atomic Absorption Determination of Volatile Hydrides Using Cold Trap CollectionAnalytical Letters, 1973
- Arsenic determination at submicrogram levels by arsine evolution and flameless atomic absorption spectrophotometric techniqueAnalytical Chemistry, 1972
- Determination of trace lead in the atmosphere by furnace atomic absorptionAnalytical Chemistry, 1972
- Gas-sampling technique for arsenic determination by atomic absorption spectrophotometryAnalytical Chemistry, 1969