Abstract
The low‐energy ion backscattering spectra of Ta2O5 obtained with He as the probe gas exhibit a pronounced low‐energy tail on the metal peak and a strong incident ion energy dependence of the oxygen to tantalum peak intensity ratio. To determine the effect differential scattering cross sections, ion neutralization, and sample reduction have on these spectral features, a combined ISS–XPS study has been carried out. The data indicate that the sample is not reduced by the He ion beam and that a resonant‐type neutralization plays a dominant role both in tailing and in the variation of the oxygen to tantalum peak intensity ratio.