Development and validation of a high‐performance liquid chromatographic procedure for the determination of herbicide residues in surface and agriculture waters
- 23 June 2003
- journal article
- research article
- Published by Wiley in Journal of Separation Science
- Vol. 26 (9-10), 935-938
- https://doi.org/10.1002/jssc.200301309
Abstract
A procedure has been developed for the determination of quinclorac, bentazone, 2,4‐D, clomazone, and propanil residues in surface and agriculture waters by SPE and HPLC‐UV. The method was validated and was applied for levels between 0.1 and 0.5 g/L, after a 500‐fold pre‐concentration. Average recoveries ranged from 85.7 to 109.8% with overall relative standard deviations of 1.8 to 13.4%.This publication has 16 references indexed in Scilit:
- Development and validation of a high-performance liquid chromatographic method for the determination of clomazone residues in surface waterJournal of Chromatography A, 2000
- Quantitation of chlorophenoxy acid herbicides by high-performance liquid chromatography with coulometric detectionJournal of Chromatography A, 1999
- Monitoring of pesticide residues and their metabolites in surface and underground waters of Imathia (N. Greece) by means of solid-phase extraction disks and gas chromatographyJournal of Chromatography A, 1998
- Pesticide chemical oxidation processes: an analytical approachTrAC Trends in Analytical Chemistry, 1997
- Monitoring of organic micropollutants in surface water by automated on-line trace-enrichment liquid and gas chromatographic systems with ultraviolet diode-array and mass spectrometric detectionJournal of Chromatography A, 1997
- Validation of chromatographic methods in biomedical analysis viewpoint and discussionJournal of Chromatography B: Biomedical Sciences and Applications, 1997
- Pesticide monitoring of drinking water with the help of solid-phase extraction and high-performance liquid chromatographyJournal of Chromatography A, 1996
- Extraction methodology and chromatography for the determination of residual pesticides in waterJournal of Chromatography A, 1996
- Determination of pesticides in environmental waters by automated on-line trace-enrichment and liquid chromatographyJournal of Chromatography A, 1994
- Solid-phase extraction followed by high-performance liquid chromatographic analysis for monitoring herbicides in drinking waterJournal of Chromatography A, 1993