Solid-state vibrational spectroscopy. Part V. An infrared and Raman spectroscopic study of metal(II) halide pyridine complexes

Abstract
Infrared (200–4 000 cm–1) and Raman (300–3 500 cm–1) spectra are reported for metal(II) halide pyridine complexes of the following stoicheiometries: [MX2(py)2](M = Mn, Fe, Co, Ni, Cu, Zn, Cd, or Hg); [MX2(py)4](M = Fe, Co, or Ni); [MX2(py)2](M = Co, Cu, Cd, or Hg); and [Hg3X6(py)2](X = Cl or Br). Structure–spectra correlations have been found for the dipyridine complexes whose structures are either monomeric tetrahedral {M = Zn or Co; X = Cl or Br; [HgBr2(py)2] and [Cdl2(py)2]}, polymeric octahedral (M = Mn, Ni, or Cd; X = Cl or Br; M = Fe or Co; X = Cl), or distorted polymeric octahedral {M = Cu, X = Cl or Br; and [HgCl2(py)2]}. For a given series of isomorphous complexes there is a correlation between the sum of the difference between the liquid and ligand values of ν2, ν3, ν4, ν5, ν6, ν7, ν8, ν9, ν10, ν17, ν27, and (ν9+ν10) and the strength of the metal–nitrogen bond as measuredbythe ν(M–N) value.