Tetrakis (Deuteriomethyl) Tetraselenafulvalene
- 1 May 1982
- journal article
- Published by Taylor & Francis in Molecular Crystals and Liquid Crystals
- Vol. 86 (1), 35-41
- https://doi.org/10.1080/00268948208073666
Abstract
The preparation of >99% D tetramethyl tetraselenafulvalene is described. The synthesis involves hydrogen deuterium exchange of biacetyl followed by conversion to d7-3-chloro-2-butanone. The latter was transformed to the title compound via known procedures. The physical properties of the salts (d12-TMTSF)2 PF 6 and (d12-TMTSF)2 ClO4 are reported.Keywords
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