A mild synthesis for tetrakis-donor-substituted molybdenum carbonyls

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Abstract
Reaction of halogenobisacetonitrile-π-allyldicarbonylmolybdenum complexes with triphenylphosphine yields thermally unstable bisacetonitriledicarbonylbis(triphenylphosphine)molybdenum(0), in which acetonitrile is easily replaced to form a series of reactive dicarbonyl-molybdenum(0) complexes.