Effect of oxygen on orientation of polycrystalline Fe films prepared by ECR-magnetron sputtering

Abstract
An ECR-magnetron sputtering system with permanent magnets has been developed and used to prepare Fe-O films. Oxygen was introduced into an Ar sputtering atmosphere during deposition of Fe onto the glass substrate. X-ray diffraction patterns of these films showed a drastic increase in intensity of the Fe(200) diffraction peak, and a rapid decrease of the Fe(110) peak. The Fe(110) single peak is observed in the film prepared without oxygen. In the films prepared with oxygen, iron oxides were not detected through x-ray diffraction, x-ray photoelectron, or magnetic properties measurements, implying that, in sputter-deposited Fe films, a small amount of oxygen brings about a [100] orientation of the Fe grains.