Bestimmung des14C-Verteilungsmusters in Glycerin

Abstract
A method is described for the determination of the intramolecular distribution of C14 in glycerol. Carbon atoms 1 and 3 of the glycerol were separately converted into formaldehyde-dimedone. Radioactivity was measured in a liquid scintillation counter. The method was shown to be suitable for the determination of the intramolecular distribution of tritium in glycerol.