Preparation and Purification of Some Oxidation Products of Perylene.

journal article
Published by National Institute of Standards and Technology (NIST) in Journal of Research of the National Bureau of Standards Section A: Physics and Chemistry

Vol. 72 (1), 39-47
https://doi.org/10.6028/jres.072A.005

Abstract

Reliable procedures are given for the purification of perylene, and for the preparation and purification of 3,10-perylenequinone, 1,12-perylenequinone, 2,11-dihydroxy-3,10-perylenequinone, 4,9-dihydroxy3,10-perylenequinone, 4-oxo-4H-benz[de]anthracene-7,8-dicarboxylic anhydride, phenanthrene 1,8,9,10-tetracarboxylic dianhydride, and anthraquinone-l,5-dicarboxylic acid. Data on the physical properties of 3,9-perylenequinone are also reported.

Keywords

4-OXY-4H-BENZ[DE]ANTHRACENE-7,8-DICARBOXYLIC ANHYDRIDE
ABSORPTION SPECTRA
AIR POLLUTANTS
ANTHRAQUINONE-L,5DICARBOXYLIC ACID
DIHYDROXYPERYLENEQUINONES
INFRARED
PERYLENE
PERYLENEQUINONES
PHOTO-OXIDATION PRODUCTS OF PERYLENE
POLYCYCLIC AROMATIC HYDROCARBONS
THIN-LAYER CHROMATOGRAMS
ULTRAVIOLET
VISIBLE ABSORPTION SPECTRA

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