The Nuclear Quadrupole Interaction of Fe57 in Spinel Type Oxides

Abstract
The nuclear quadrupole interaction of Fe 57 in spinel type oxides was investigated by means of Mössbauer experiments of the 14.4 keV gamma rays from Fe 57m . On octahedral sites in ZnFe 2 O 4 , a spectrum split symmetrically into two lines was observed in paramagnetic state, which is attributed to the nuclear quadrupole splitting in ferric ions arising from the trigonal field on B site. As for tetrahedral sites of the spinel structure, similar spectra to the former case were observed in FeNiAlO 4 and FeNiCrO 4 . The origin of the quadrupole interaction in these samples is considered to be due to the distribution of divalent and trivalent ions on B sites which establishes the local charge neutrality. In FeAl 2 O 4 , which has homogeneous B sites, only one sharp absorption dip was observed.