The Application of 13C‐NMR Spectroscopy to Study Lipid A from Yersinia pseudotuberculosis Lipopolysaccharide
- 1 August 1982
- journal article
- research article
- Published by Wiley in European Journal of Biochemistry
- Vol. 126 (2), 349-351
- https://doi.org/10.1111/j.1432-1033.1982.tb06786.x
Abstract
The use of 13C-NMR spectroscopy in the establishment of lipid A backbone structure from lipopolysaccharide of Y. pseudotuberculosis is described. The 13C-NMR spectra of degraded lipid A and its N-acetate were obtained. The assignment of signals was made by comparison with the chemical shifts for 13C-NMR spectra of glucosaminitol, N-acetyl-glucosaminitol and their .beta.-1,4 and .beta.-1,6-disaccharides. The lipid A backbone of the lipopolysaccharide in question consists of .beta.-1,6-linked glucosamine disaccharide.This publication has 7 references indexed in Scilit:
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