A CONVENIENT ONE-POT SYNTHESIS OF STANNYLSILANES
- 1 April 1997
- journal article
- research article
- Published by Taylor & Francis in Phosphorus, Sulfur, and Silicon and the Related Elements
- Vol. 123 (1), 255-261
- https://doi.org/10.1080/10426509708044214
Abstract
Stannylsilanes were synthesized in high yields by reaction of organotinchlorides with organofluorosilanes and magnesium. The fluorosilanes were prepared in good yields and under mild conditions by reaction of the corresponding chlorosilanes with [n-Bu4N][Ph3SnF2]. All products were characterized by 29Si, 119Sn NMR spectroscopy and elemental analysis.Keywords
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